3D核磁共振实验的相对灵敏度

三维实验的灵敏度列表

ExperimentAssignmentCommentRelative S/N[%]
HNCOH(i)-N(i)-C’(i-1)<20 kD, above use 2H labeling100
HNCAH(i)-N(i)-Ca(i)Ca(i-1)<20 kD, above use 2H labeling50/15
HN(Co)CAH(i)-N(i)-Ca(i-1)<20 kD, above use 2H labeling71
HN(CA)CoH(i)-N(i)-C’(i)<20 kD, above use 2H labeling13/4
CBCA(Co)NHH(i)-N(i)-Ca(i-1)Cb(i-1)<20 kD, above use 2H labeling13/9 a/b
HBHA(Co)NHH(i)-N(i)-Ha(i-1)Hb(i-1)<20 kD, above use 2H labeling13/9 a/b
CBCANH,HNCACBH(i)-N(i)-Ca(i-1)Ca(i)Cb(i-1)Cb(i)<15 kD, above use 2H labeling4/1.7 a/b(i), 1.3/0.5 a/b(i-1)
(H)CC(Co)NH-TocsyH(i)-N(i)-Caliph(i-1)<15-20 kD, above use 2H labeling
H(CC)(Co)NH-TocsyH(i)-N(i)-Caliph(i-1)<15-20 kD, above use 2H labeling
HCCH-TocsyHaliph-Caliph<25 kD, sensitive, but tedious to analyze, combine with HCCONH type exp